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https://doi.org/10.5562/cca2111

Controlling Solvate Formation of a Schiff Base by Combining Mechano-chemistry with Solution Synthesis

Vladimir Stilinović ; Department of Chemistry, Laboratory of General and Inorganic Chemistry,Faculty of Science, Horvatovac 102a, University of Zagreb, 10000 Zagreb, Croatia
Dominik Cinčić ; Department of Chemistry, Laboratory of General and Inorganic Chemistry,Faculty of Science, Horvatovac 102a, University of Zagreb, 10000 Zagreb, Croatia
Marija Zbačnik ; Department of Chemistry, Laboratory of General and Inorganic Chemistry,Faculty of Science, Horvatovac 102a, University of Zagreb, 10000 Zagreb, Croatia
Branko Kaitner ; Department of Chemistry, Laboratory of General and Inorganic Chemistry,Faculty of Science, Horvatovac 102a, University of Zagreb, 10000 Zagreb, Croatia

Puni tekst: engleski, pdf (4 MB) str. 485-493 preuzimanja: 1.389* citiraj
APA 6th Edition
Stilinović, V., Cinčić, D., Zbačnik, M. i Kaitner, B. (2012). Controlling Solvate Formation of a Schiff Base by Combining Mechano-chemistry with Solution Synthesis. Croatica Chemica Acta, 85 (4), 485-493. https://doi.org/10.5562/cca2111
MLA 8th Edition
Stilinović, Vladimir, et al. "Controlling Solvate Formation of a Schiff Base by Combining Mechano-chemistry with Solution Synthesis." Croatica Chemica Acta, vol. 85, br. 4, 2012, str. 485-493. https://doi.org/10.5562/cca2111. Citirano 26.02.2021.
Chicago 17th Edition
Stilinović, Vladimir, Dominik Cinčić, Marija Zbačnik i Branko Kaitner. "Controlling Solvate Formation of a Schiff Base by Combining Mechano-chemistry with Solution Synthesis." Croatica Chemica Acta 85, br. 4 (2012): 485-493. https://doi.org/10.5562/cca2111
Harvard
Stilinović, V., et al. (2012). 'Controlling Solvate Formation of a Schiff Base by Combining Mechano-chemistry with Solution Synthesis', Croatica Chemica Acta, 85(4), str. 485-493. https://doi.org/10.5562/cca2111
Vancouver
Stilinović V, Cinčić D, Zbačnik M, Kaitner B. Controlling Solvate Formation of a Schiff Base by Combining Mechano-chemistry with Solution Synthesis. Croatica Chemica Acta [Internet]. 2012 [pristupljeno 26.02.2021.];85(4):485-493. https://doi.org/10.5562/cca2111
IEEE
V. Stilinović, D. Cinčić, M. Zbačnik i B. Kaitner, "Controlling Solvate Formation of a Schiff Base by Combining Mechano-chemistry with Solution Synthesis", Croatica Chemica Acta, vol.85, br. 4, str. 485-493, 2012. [Online]. https://doi.org/10.5562/cca2111

Sažetak
A Schiff base dicarboxylic acid (1) was prepared by condensation of 2-hydroxy-1-naphthaldehyde with 5-aminoisophthalic acid. Its solvates with pyridine (2a and 2b) and dimethylformamide (3) were prepared by liquid-assisted grinding and by conventional solvent-based methods. All products were characterised by FT-IR spectroscopy, thermogravimetric analysis and differential scanning calorimetry. The structures of 1, 2b and 3 were determined by single crystal X-ray diffraction. 1 was found to be a pure Schiff base, 2b a pyridine solvate and 3 a dimethylformamide solvate monohydrate. In all three structures, the Schiff base molecule appears to be present as the ketoamine tautomer.(doi: 10.5562/cca2111)

Ključne riječi
Schiff base; solvates; dicarboxylic acid; mechanochemistry; tautomerism

Hrčak ID: 94446

URI
https://hrcak.srce.hr/94446

Posjeta: 1.802 *