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Acyclic Analogues of Purine Nucleosides with Dimethylaminoethyl and Dimethylaminoethoxyalkyl Side Chains: Preparation, One- and Two-dimensional 1H- and 13C-NMR Studies

Mario Pongračić ; Pliva Research Institute, Prilaz Baruna Filipovića 25, 10000 Zagreb, Croatia
Silvana Raić ; Department of Organic Chemistry, Faculty of Chemical Engineering and Technology, University of Zagreb, Maruličev trg 20, 10000 Zagreb, Croatia
Dražen Vìkić-Topić ; Ruđer Bošković Institute, NMR Laboratory, HR-10001 Zagreb, Croatia
Mladen Mintas ; Department of Organic Chemistry, Faculty of Chemical Engineering and Technology, University of Zagreb, Maruličev trg 20, 10000 Zagreb, Croatia

Puni tekst: engleski, pdf (22 MB) str. 1047-1062 preuzimanja: 110* citiraj
APA 6th Edition
Pongračić, M., Raić, S., Vìkić-Topić, D. i Mintas, M. (1997). Acyclic Analogues of Purine Nucleosides with Dimethylaminoethyl and Dimethylaminoethoxyalkyl Side Chains: Preparation, One- and Two-dimensional 1H- and 13C-NMR Studies. Croatica Chemica Acta, 70 (4), 1047-1062. Preuzeto s https://hrcak.srce.hr/135659
MLA 8th Edition
Pongračić, Mario, et al. "Acyclic Analogues of Purine Nucleosides with Dimethylaminoethyl and Dimethylaminoethoxyalkyl Side Chains: Preparation, One- and Two-dimensional 1H- and 13C-NMR Studies." Croatica Chemica Acta, vol. 70, br. 4, 1997, str. 1047-1062. https://hrcak.srce.hr/135659. Citirano 28.10.2020.
Chicago 17th Edition
Pongračić, Mario, Silvana Raić, Dražen Vìkić-Topić i Mladen Mintas. "Acyclic Analogues of Purine Nucleosides with Dimethylaminoethyl and Dimethylaminoethoxyalkyl Side Chains: Preparation, One- and Two-dimensional 1H- and 13C-NMR Studies." Croatica Chemica Acta 70, br. 4 (1997): 1047-1062. https://hrcak.srce.hr/135659
Harvard
Pongračić, M., et al. (1997). 'Acyclic Analogues of Purine Nucleosides with Dimethylaminoethyl and Dimethylaminoethoxyalkyl Side Chains: Preparation, One- and Two-dimensional 1H- and 13C-NMR Studies', Croatica Chemica Acta, 70(4), str. 1047-1062. Preuzeto s: https://hrcak.srce.hr/135659 (Datum pristupa: 28.10.2020.)
Vancouver
Pongračić M, Raić S, Vìkić-Topić D, Mintas M. Acyclic Analogues of Purine Nucleosides with Dimethylaminoethyl and Dimethylaminoethoxyalkyl Side Chains: Preparation, One- and Two-dimensional 1H- and 13C-NMR Studies. Croatica Chemica Acta [Internet]. 1997 [pristupljeno 28.10.2020.];70(4):1047-1062. Dostupno na: https://hrcak.srce.hr/135659
IEEE
M. Pongračić, S. Raić, D. Vìkić-Topić i M. Mintas, "Acyclic Analogues of Purine Nucleosides with Dimethylaminoethyl and Dimethylaminoethoxyalkyl Side Chains: Preparation, One- and Two-dimensional 1H- and 13C-NMR Studies", Croatica Chemica Acta, vol.70, br. 4, str. 1047-1062, 1997. [Online]. Dostupno na: https://hrcak.srce.hr/135659. [Citirano: 28.10.2020.]

Sažetak
The novel acyclic analogues of purine nucleosides containing 6-N- [2-(dimethylamino)ethyl] and 9-(2-hydroxyalkyl) substituents (6, 7), or 9-[2-(2-(dimethylamino)ethoxy)alkyl] substituent and 6-amino group, free (5) or transformed into pyrrolo moiety (11, 12), were prepared by reaction of protected 9-(2-hydroxyalkyl)adenines with 2-(dimethylamino)ethyl chloride hydrochloride. The substitution site in the purine ring was determined by 1H- and 13C-NMR, using chemical and substituent induced shifts, H-H and C-H coupling constants and connectivities in two-dimensional homo- and hetero- nuclear correlation spectra.

Hrčak ID: 135659

URI
https://hrcak.srce.hr/135659

Posjeta: 214 *