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Crystal and Molecular Structure of (S)-a-(pCyanobenzenesulphonamido)-B- propiothiolactone, C10H8N203S2

Ivanka Matijašić ; Laboratory of Organic Chemistry and Biochemistry, Faculty of Science, University of Zagreb, Strossmayerov trg 14, Zagreb
Giovanni D. Andreetti ; Istituto di Strutturistica Chimica, Universita di Parma, C. N. R., Centro di Studio per la Strutturistica Diffrattometrica, Parma, Italy
Paolo Sgarabotto ; Istituto di Strutturistica Chimica, Universita di Parma, C. N. R., Centro di Studio per la Strutturistica Diffrattometrica, Parma, Italy
Aleksandar Bezjak ; Department of Chemistry, Faculty of Pharmacy and Biochemistry, University of Zagreb, Zagreb
Dragutin Fleš ; Research and Development Institute INA, Zagreb, Yugoslavia

Puni tekst: engleski, pdf (3 MB) str. 285-291 preuzimanja: 83* citiraj
APA 6th Edition
Matijašić, I., Andreetti, G.D., Sgarabotto, P., Bezjak, A. i Fleš, D. (1987). Crystal and Molecular Structure of (S)-a-(pCyanobenzenesulphonamido)-B- propiothiolactone, C10H8N203S2. Croatica Chemica Acta, 60 (2), 285-291. Preuzeto s https://hrcak.srce.hr/176356
MLA 8th Edition
Matijašić, Ivanka, et al. "Crystal and Molecular Structure of (S)-a-(pCyanobenzenesulphonamido)-B- propiothiolactone, C10H8N203S2." Croatica Chemica Acta, vol. 60, br. 2, 1987, str. 285-291. https://hrcak.srce.hr/176356. Citirano 28.02.2021.
Chicago 17th Edition
Matijašić, Ivanka, Giovanni D. Andreetti, Paolo Sgarabotto, Aleksandar Bezjak i Dragutin Fleš. "Crystal and Molecular Structure of (S)-a-(pCyanobenzenesulphonamido)-B- propiothiolactone, C10H8N203S2." Croatica Chemica Acta 60, br. 2 (1987): 285-291. https://hrcak.srce.hr/176356
Harvard
Matijašić, I., et al. (1987). 'Crystal and Molecular Structure of (S)-a-(pCyanobenzenesulphonamido)-B- propiothiolactone, C10H8N203S2', Croatica Chemica Acta, 60(2), str. 285-291. Preuzeto s: https://hrcak.srce.hr/176356 (Datum pristupa: 28.02.2021.)
Vancouver
Matijašić I, Andreetti GD, Sgarabotto P, Bezjak A, Fleš D. Crystal and Molecular Structure of (S)-a-(pCyanobenzenesulphonamido)-B- propiothiolactone, C10H8N203S2. Croatica Chemica Acta [Internet]. 1987 [pristupljeno 28.02.2021.];60(2):285-291. Dostupno na: https://hrcak.srce.hr/176356
IEEE
I. Matijašić, G.D. Andreetti, P. Sgarabotto, A. Bezjak i D. Fleš, "Crystal and Molecular Structure of (S)-a-(pCyanobenzenesulphonamido)-B- propiothiolactone, C10H8N203S2", Croatica Chemica Acta, vol.60, br. 2, str. 285-291, 1987. [Online]. Dostupno na: https://hrcak.srce.hr/176356. [Citirano: 28.02.2021.]

Sažetak
Crystals of the title compound are monoclinic, space group
P21, with a = 1.0018(2), b = 0.9722(2), c = 0.6262(1) nm, fJ = 102.32(1)° and Z = 2. The structure was solved by direct methods using 1113 reflections with I 2': 20 (I) and refined to a conventional R index
of 0.051. The heterocyclic four-membered ring is bent and has a
puckering angle of 18.7(7)°. The dihedral angle between the best
planes of the B-propiothiolactone and benzene ring is 70.2(3)°.
Discrete molecules are connected along the b axis by intermolecular
hydrogen bonds N--H ... O of 309.5(9) pm.

Hrčak ID: 176356

URI
https://hrcak.srce.hr/176356

Posjeta: 161 *