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Original scientific paper

The Crystal Structure of Pyridinium μ-salicylato-tetrachloro-μ- oxo-μ-ethoxo-dioxodimolibdate(V)

Boris Kamenar ; Laboratory of General and Inorganic Chemistry, Faculty of Science, University of Zagreb, P. 0. Box 153, 41001 Zagreb, Yugoslavia
Maja Penavić ; Laboratory of General and Inorganic Chemistry, Faculty of Science, University of Zagreb, P. 0. Box 153, 41001 Zagreb, Yugoslavia
Berislav Marković ; Laboratory of General and Inorganic Chemistry, Faculty of Science, University of Zagreb, P. 0. Box 153, 41001 Zagreb, Yugoslavia

Fulltext: english, pdf (8 MB) pages 637-643 downloads: 85* cite
APA 6th Edition
Kamenar, B., Penavić, M. & Marković, B. (1984). The Crystal Structure of Pyridinium μ-salicylato-tetrachloro-μ- oxo-μ-ethoxo-dioxodimolibdate(V). Croatica Chemica Acta, 57 (4), 637-643. Retrieved from https://hrcak.srce.hr/194132
MLA 8th Edition
Kamenar, Boris, et al. "The Crystal Structure of Pyridinium μ-salicylato-tetrachloro-μ- oxo-μ-ethoxo-dioxodimolibdate(V)." Croatica Chemica Acta, vol. 57, no. 4, 1984, pp. 637-643. https://hrcak.srce.hr/194132. Accessed 27 Jul. 2021.
Chicago 17th Edition
Kamenar, Boris, Maja Penavić and Berislav Marković. "The Crystal Structure of Pyridinium μ-salicylato-tetrachloro-μ- oxo-μ-ethoxo-dioxodimolibdate(V)." Croatica Chemica Acta 57, no. 4 (1984): 637-643. https://hrcak.srce.hr/194132
Harvard
Kamenar, B., Penavić, M., and Marković, B. (1984). 'The Crystal Structure of Pyridinium μ-salicylato-tetrachloro-μ- oxo-μ-ethoxo-dioxodimolibdate(V)', Croatica Chemica Acta, 57(4), pp. 637-643. Available at: https://hrcak.srce.hr/194132 (Accessed 27 July 2021)
Vancouver
Kamenar B, Penavić M, Marković B. The Crystal Structure of Pyridinium μ-salicylato-tetrachloro-μ- oxo-μ-ethoxo-dioxodimolibdate(V). Croatica Chemica Acta [Internet]. 1984 [cited 2021 July 27];57(4):637-643. Available from: https://hrcak.srce.hr/194132
IEEE
B. Kamenar, M. Penavić and B. Marković, "The Crystal Structure of Pyridinium μ-salicylato-tetrachloro-μ- oxo-μ-ethoxo-dioxodimolibdate(V)", Croatica Chemica Acta, vol.57, no. 4, pp. 637-643, 1984. [Online]. Available: https://hrcak.srce.hr/194132. [Accessed: 27 July 2021]

Abstracts
The crystal structure of the title complex has been determined
from diffractometer X-ray intensity data by means of Patterson ·
and Fourier methods and refined by the full matrix least-squares
technique to an R index of 0.060 (Rw = 0.064). The crystals are
built up of pyH+ cations and [Mo20sCl4 (C2HsO) (HOC6H4C02)J2-
anions. Each molybdenum atom of the binuclear anion is octahedrally
coordinated, being bonded to two oxo-oxygen atoms, one
terminal (1.669 and 1.670 A) and one bridging (1.908 and 1.916 A),
one bridging ethoxo-oxygen atom (1.963 and 1.964 A), one salicylato-
oxygen atom (2.295 and 2.317 A) and two chlorine atoms
(from 2.399 to 2.432 A). The terminal oxo-oxygens occupy a cis-
position with respect to the Mo20 2 bridge. The dihedral angle
between the two Mo02 planes within the bridge amounts to 164.9°.
The Mo-Mo bond lengths is 2.646A.

Hrčak ID: 194132

URI
https://hrcak.srce.hr/194132

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