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https://doi.org/10.15255/KUI.2018.021

Mechanochemical Synthesis of Calcium Oxalate

Silvija Šafranko ; Department of Chemistry, University of Osijek, Ulica cara Hadrijana 8A, 31 000 Osijek, Croatia
Dominik Goman ; Department of Chemistry, University of Osijek, Ulica cara Hadrijana 8A, 31 000 Osijek, Croatia
Filip Bolić ; Department of Chemistry, University of Osijek, Ulica cara Hadrijana 8A, 31 000 Osijek, Croatia
Marina Sekulić ; Department of Chemistry, University of Osijek, Ulica cara Hadrijana 8A, 31 000 Osijek, Croatia
Anamarija Stanković ; Department of Chemistry, University of Osijek, Ulica cara Hadrijana 8A, 31 000 Osijek, Croatia
Nives Matijaković ; Ruđer Bošković Institute, Laboratory for precipitation processes, Bijenička cesta 54, 10 000 Zagreb, Croatia
Ina Erceg ; Ruđer Bošković Institute, Laboratory for biocolloids and surface chemistry, Bijenička cesta 54, 10 000 Zagreb, Croatia
Berislav Marković ; Department of Chemistry, University of Osijek, Ulica cara Hadrijana 8A, 31 000 Osijek, Croatia

Puni tekst: hrvatski, pdf (2 MB) str. P73-P83 preuzimanja: 96* citiraj
APA 6th Edition
Šafranko, S., Goman, D., Bolić, F., Sekulić, M., Stanković, A., Matijaković, N., ... Marković, B. (2018). Mehanokemijska sinteza kalcijeva oksalata. Kemija u industriji, 67 (13 (special issue)), P73-P83. https://doi.org/10.15255/KUI.2018.021
MLA 8th Edition
Šafranko, Silvija, et al. "Mehanokemijska sinteza kalcijeva oksalata." Kemija u industriji, vol. 67, br. 13 (special issue), 2018, str. P73-P83. https://doi.org/10.15255/KUI.2018.021. Citirano 12.11.2019.
Chicago 17th Edition
Šafranko, Silvija, Dominik Goman, Filip Bolić, Marina Sekulić, Anamarija Stanković, Nives Matijaković, Ina Erceg i Berislav Marković. "Mehanokemijska sinteza kalcijeva oksalata." Kemija u industriji 67, br. 13 (special issue) (2018): P73-P83. https://doi.org/10.15255/KUI.2018.021
Harvard
Šafranko, S., et al. (2018). 'Mehanokemijska sinteza kalcijeva oksalata', Kemija u industriji, 67(13 (special issue)), str. P73-P83. https://doi.org/10.15255/KUI.2018.021
Vancouver
Šafranko S, Goman D, Bolić F, Sekulić M, Stanković A, Matijaković N i sur. Mehanokemijska sinteza kalcijeva oksalata. Kemija u industriji [Internet]. 2018 [pristupljeno 12.11.2019.];67(13 (special issue)):P73-P83. https://doi.org/10.15255/KUI.2018.021
IEEE
S. Šafranko, et al., "Mehanokemijska sinteza kalcijeva oksalata", Kemija u industriji, vol.67, br. 13 (special issue), str. P73-P83, 2018. [Online]. https://doi.org/10.15255/KUI.2018.021

Sažetak
In this work, mechanochemical synthesis of calcium oxalate was done in a planetary ball mill, with and without addition of water as a solvent. Previous research was primarily focused on calcium oxalate synthesis in solution. Here we report a different approach which may contribute to new findings in calcium oxalate crystal synthesis caused by an influence of mechanical energy.
The aim of this study was synthesis, identification, and characterization of particular oxalate hydrate phase synthesized with calcium salts (chloride, nitrate and sulphate). The effects of grinding speed and reaction duration regarding the time of synthesis were investigated. Structural and thermal sample properties were studied by FTIR spectroscopy and thermogravimetric analysis (TGA). Morphologic characteristics of calcium oxalate and size distribution were measured by optical microscopy and dynamic light scattering (DLS).

Creative Commons License
This work is licensed under a Creative Commons Attribution 4.0 International License.

Ključne riječi
mechanochemistry; calcium oxalate monohydrate; kidney stones

Hrčak ID: 207070

URI
https://hrcak.srce.hr/207070

[hrvatski]

Posjeta: 197 *