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Synthetic Studies in the Chloramphenicol Series. VI. Synthesis of DL - threo-1-p-nitrophenyl-1 -hydroxy-2-dichloroacetamido-3- methylsulfinyl and 3-methylsulfonyl propane

M. Fleš ; Research Department, »Pliva« Pharmaceutical and Chemical Works, Zagreb, Croatia, Yugoslavia

Puni tekst: engleski, pdf (7 MB) str. 257-262 preuzimanja: 40* citiraj
APA 6th Edition
Fleš, M. (1963). Synthetic Studies in the Chloramphenicol Series. VI. Synthesis of DL - threo-1-p-nitrophenyl-1 -hydroxy-2-dichloroacetamido-3- methylsulfinyl and 3-methylsulfonyl propane. Croatica Chemica Acta, 35 (4), 257-262. Preuzeto s https://hrcak.srce.hr/208323
MLA 8th Edition
Fleš, M.. "Synthetic Studies in the Chloramphenicol Series. VI. Synthesis of DL - threo-1-p-nitrophenyl-1 -hydroxy-2-dichloroacetamido-3- methylsulfinyl and 3-methylsulfonyl propane." Croatica Chemica Acta, vol. 35, br. 4, 1963, str. 257-262. https://hrcak.srce.hr/208323. Citirano 08.03.2021.
Chicago 17th Edition
Fleš, M.. "Synthetic Studies in the Chloramphenicol Series. VI. Synthesis of DL - threo-1-p-nitrophenyl-1 -hydroxy-2-dichloroacetamido-3- methylsulfinyl and 3-methylsulfonyl propane." Croatica Chemica Acta 35, br. 4 (1963): 257-262. https://hrcak.srce.hr/208323
Harvard
Fleš, M. (1963). 'Synthetic Studies in the Chloramphenicol Series. VI. Synthesis of DL - threo-1-p-nitrophenyl-1 -hydroxy-2-dichloroacetamido-3- methylsulfinyl and 3-methylsulfonyl propane', Croatica Chemica Acta, 35(4), str. 257-262. Preuzeto s: https://hrcak.srce.hr/208323 (Datum pristupa: 08.03.2021.)
Vancouver
Fleš M. Synthetic Studies in the Chloramphenicol Series. VI. Synthesis of DL - threo-1-p-nitrophenyl-1 -hydroxy-2-dichloroacetamido-3- methylsulfinyl and 3-methylsulfonyl propane. Croatica Chemica Acta [Internet]. 1963 [pristupljeno 08.03.2021.];35(4):257-262. Dostupno na: https://hrcak.srce.hr/208323
IEEE
M. Fleš, "Synthetic Studies in the Chloramphenicol Series. VI. Synthesis of DL - threo-1-p-nitrophenyl-1 -hydroxy-2-dichloroacetamido-3- methylsulfinyl and 3-methylsulfonyl propane", Croatica Chemica Acta, vol.35, br. 4, str. 257-262, 1963. [Online]. Dostupno na: https://hrcak.srce.hr/208323. [Citirano: 08.03.2021.]

Sažetak
The compounds mentioned in the title were prepared from
a.-phthalimido-~-methylmercaptopropiophenone (I). Reduction of
I with aluminium isopropoxide gave preferentially the threo carbinol
II which upon acetylation and subsequent nitration gave
a mixture of diastereomeric sulfoxides which were oxidized with
hydrogen peroxide to the identical sulfones.

Hrčak ID: 208323

URI
https://hrcak.srce.hr/208323

Posjeta: 76 *