hrcak mascot   Srce   HID

Izvorni znanstveni članak
https://doi.org/10.5599/jese.676

Electrodeposition of the Sb2Se3 thin films on various substrates from the tartaric electrolyte

Vusala Asim Majidzade   ORCID icon orcid.org/0000-0001-5639-3104 ; M. Nagıyev Azerbaijan National Academy of Sciences (ANAS), Baku, AZ1143, Azerbaijan
Akif Shikhan Aliyev   ORCID icon orcid.org/0000-0003-0560-5263 ; M. Nagıyev Azerbaijan National Academy of Sciences (ANAS), Baku, AZ1143, Azerbaijan
Parvin Heydar Guliyev ; Nakchivan State University, Nakchivan AR, AZ 7012, Azerbaijan
Dunya Mahammad Babanly ; M. Nagıyev Azerbaijan National Academy of Sciences (ANAS), Baku, AZ1143, Azerbaijan

Puni tekst: engleski, pdf (684 KB) str. 1-9 preuzimanja: 152* citiraj
APA 6th Edition
Majidzade, V.A., Shikhan Aliyev, A., Heydar Guliyev, P. i Mahammad Babanly, D. (2020). Electrodeposition of the Sb2Se3 thin films on various substrates from the tartaric electrolyte. Journal of Electrochemical Science and Engineering, 10 (1), 1-9. https://doi.org/10.5599/jese.676
MLA 8th Edition
Majidzade, Vusala Asim, et al. "Electrodeposition of the Sb2Se3 thin films on various substrates from the tartaric electrolyte." Journal of Electrochemical Science and Engineering, vol. 10, br. 1, 2020, str. 1-9. https://doi.org/10.5599/jese.676. Citirano 27.07.2021.
Chicago 17th Edition
Majidzade, Vusala Asim, Akif Shikhan Aliyev, Parvin Heydar Guliyev i Dunya Mahammad Babanly. "Electrodeposition of the Sb2Se3 thin films on various substrates from the tartaric electrolyte." Journal of Electrochemical Science and Engineering 10, br. 1 (2020): 1-9. https://doi.org/10.5599/jese.676
Harvard
Majidzade, V.A., et al. (2020). 'Electrodeposition of the Sb2Se3 thin films on various substrates from the tartaric electrolyte', Journal of Electrochemical Science and Engineering, 10(1), str. 1-9. https://doi.org/10.5599/jese.676
Vancouver
Majidzade VA, Shikhan Aliyev A, Heydar Guliyev P, Mahammad Babanly D. Electrodeposition of the Sb2Se3 thin films on various substrates from the tartaric electrolyte. Journal of Electrochemical Science and Engineering [Internet]. 2020 [pristupljeno 27.07.2021.];10(1):1-9. https://doi.org/10.5599/jese.676
IEEE
V.A. Majidzade, A. Shikhan Aliyev, P. Heydar Guliyev i D. Mahammad Babanly, "Electrodeposition of the Sb2Se3 thin films on various substrates from the tartaric electrolyte", Journal of Electrochemical Science and Engineering, vol.10, br. 1, str. 1-9, 2020. [Online]. https://doi.org/10.5599/jese.676

Sažetak
The present contribution is devoted to the electrochemical deposition of Sb2Se3 thin films from tartrate electrolyte. The study was conducted by potentiodynamic, potentiostatic and galvanostatic methods carried out under different conditions at Pt, Cu and Ni electrodes.
The kinetics and mechanism of the electroreduction of antimony and selenite ions in the tartaric acid were studied separately for the electrochemical deposition. Comparison of the obtained polarization curves showed that co-deposition occurs between electroreduction
potentials of antimony and selenium, indicating depolarization electrode effect for antimony ions. The influence of electrolyte composition, pH, current density, temperature, etc. has been studied. On the basis of cyclic polarization, X-ray phase and SEM-EDX analyses,
it is found that Sb-Se thin films are deposited on Pt and Ni electrodes, but not on Cu electrode. Black, uniform, crystalline and shiny films of the stoichiometric composition of Sb2Se3 compound are deposited on Pt and Ni electrodes within the 338-348 K temperature interval, pH 1.85, current density of 2.5-3.0 A/dm2, and annealing temperature of 703 K. Experiments were carried out using the optimal electrolyte composition containing 0.05 M SbOCl + 0.05 M H2SeO3 + 0.007 M C4H6O6.

Ključne riječi
Antimony triselenide; semiconductor; electrochemical deposition; polarization; tartaric acid

Hrčak ID: 229461

URI
https://hrcak.srce.hr/229461

Posjeta: 324 *