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https://doi.org/10.5562/cca2381

Direct and Facile Synthesis of Acyl Isothiocyanates from Carboxylic Acids Using Trichloroisocyanuric Acid/Triphenylphosphine System

Najmeh Entezari ; Department of Chemistry, Faculty of Sciences, Ferdowsi University of Mashhad, Mashhad 9177948974, Iran
Batool Akhlaghinia orcid id orcid.org/0000-0002-9940-5045 ; Department of Chemistry, Faculty of Sciences, Ferdowsi University of Mashhad, Mashhad 9177948974, Iran
Hamed Rouhi-Saadabad ; Department of Chemistry, Faculty of Sciences, Ferdowsi University of Mashhad, Mashhad 9177948974, Iran


Puni tekst: engleski pdf 2.813 Kb

str. 201-206

preuzimanja: 2.778

citiraj


Sažetak

A mild, efficient, and practical method for one-step synthesis of alkanoyl and aroyl isothiocyanates from carboxylic acids using a safe and inexpensive mixed reagent, trichloroisocyanuric acid/triphenyl¬phosphine is described at room temperature. Availability of the reagents and easy workup of the reaction make this method attractive for organic chemists.

Ključne riječi

acyl isothiocyanates, carboxylic acids, trichloroisocyanuric acid (TCCA), triphenylphosphine (TPP), potassium thiocyanate

Hrčak ID:

130427

URI

https://hrcak.srce.hr/130427

Posjeta: 3.312 *