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Substituent Effect on the Association Equilibria of Free Radical Anions. Electrochemical Reduction of p-Substituted Nitrobenzenes in N,N-Dimethylformamide

Barbara Kwiatek ; Department of Chemistry, University of Warsaw, 1 Pusteur St. 02-093 Warszawa, Poland
Marek K. Kalinowski ; Department of Chemistry, University of Warsaw, 1 Pusteur St. 02-093 Warszawa, Poland


Puni tekst: engleski pdf 2.530 Kb

str. 901-906

preuzimanja: 336

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Sažetak

Association constants between p-substituted nitrobenzene anion radicals, formed by reduction of the parent molecules at a dropping mercuryelectrode, and tetraethylammonium cation in
N,N-dimethylformamide have been determined by studying the
variation in the half-wave potential with solution composition.
The association constant was observed to depend on the substituent
effect; it was shown that the Hammett equation in the form log K" = - 1.550 + 2.77 is fulfilled.The dependence of logK" vs. the hyperfine splitting constant (from ESR spectra) proper for N-nuclei in nitro-group of radical anions is also discussed.

Ključne riječi

Hrčak ID:

177275

URI

https://hrcak.srce.hr/177275

Datum izdavanja:

5.11.1986.

Posjeta: 748 *