Croatica Chemica Acta, Vol. 82 No. 2, 2009.
Izvorni znanstveni članak
A New Portable XRD/XRF Instrument for Non-destructive Analysis
Augusto Pifferi
; Istituto di Cristallografia, CNR, sezione di Monterotondo, Area della Ricerca di Roma - Montelibretti, P. O. Box 10, 00016 Monterotondo St.(RM), Italy
Gaetano Campi
; Istituto di Cristallografia, CNR, via G. Amendola 122, 70126 Bari, Italy
Carmelo Giacovazzo
; Istituto di Cristallografia, CNR, via G. Amendola 122, 70126 Bari, Italy
Ettore Gobbi
; Assing S. P. A. via E. Amaldi 14, 00016 Monterotondo (Roma), Italy
Sažetak
A new integrated portable apparatus capable of in situ X-ray diffraction (XRD) and X-ray fluorescence (XRF) measurements is presented. The instrument equipment is based on a Theta-Theta horizontal goniometer projected and developed in order to optimize stability and reliability for apparatus of such a reduced size and capable of capturing both XRF and XRD information. The simultaneous XRD/XRF data collection is achieved by using a Si solid state detector counting the X-ray photons scattered from the sample as a function of both the energy and the angular step. The instrument is also equipped with a software developed in order to provide both ease of operation in the data collection and a complete and fast characterization of the materials in the data analysis.
Ključne riječi
diffractometers; X-ray fluorescence; X-ray diffraction; data acquisition; data analysis
Hrčak ID:
39662
URI
Datum izdavanja:
15.7.2009.
Posjeta: 4.229 *