Croatica Chemica Acta, Vol. 37 No. 4, 1965.
Original scientific paper
Correction of Preferential Crystallite Orientation in X-ray Quantitative Analysis. Quantitative X:ray Determination of Ca (OH)2
A. Bezjak
; Research Department, Association of Yugoslav Cement Producers, Zagreb , Croatia, Yugoslavia
I. Jelenić
; Research Department, Association of Yugoslav Cement Producers, Zagreb , Croatia, Yugoslavia
Abstract
The work deals with the problem of preferential orientation
of crystallites in quantitafrwe X-ray analysis. A n ew method has
been worked out theoretically. and practically for the correction
of reflection intensities from 'polycrystalline samples w ith preferentially
oriented crystallites. Equations are included for the
determination of correction parameters. Practical a pplication of
the new method is demonstrated on quantitative X-ray analysis of
calcium hydroxide. The work includes a calibration graph for the
determination of coefficient a, comparing corrected and uncorrecte
d values of analytical intensities of Ca(OH)2.
Keywords
Hrčak ID:
208196
URI
Publication date:
31.3.1966.
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