Croatica Chemica Acta, Vol. 34 No. 3, 1962.
Short communication, Note
On the Synthesis of and Magnetic Measurements on Xenon Tetrafluoride
J. Slivnik
; »Jozef Stefan« Institute for Nuclear Research, Ljubljana, Slovenia, Yugoslavia
B. Brčić
; »Jozef Stefan« Institute for Nuclear Research, Ljubljana, Slovenia, Yugoslavia
B. Volavšek
; »Jozef Stefan« Institute for Nuclear Research, Ljubljana, Slovenia, Yugoslavia
A. Šmalc
; »Jozef Stefan« Institute for Nuclear Research, Ljubljana, Slovenia, Yugoslavia
B. Frlec
; »Jozef Stefan« Institute for Nuclear Research, Ljubljana, Slovenia, Yugoslavia
R. Zemljič
; »Jozef Stefan« Institute for Nuclear Research, Ljubljana, Slovenia, Yugoslavia
A. Anžur
; »Jozef Stefan« Institute for Nuclear Research, Ljubljana, Slovenia, Yugoslavia
Z. Veksli
; Institute »Ruder BoskoviC«, Zagreb, Croatia, Yugoslavia
Abstract
Recently the synthesis of XeF4 was reported from the Argonne Nationlll
Laborato·ry, and some of its physical properties were given1• In order to
obtalin further information on this extraordinarily interesting compound
XeF4 was prepared in our laboratory. Siince the details of the synthesis
were not available the direct fluorination was performed under pressure at
400°C. The basic .idea was to obtain the maximum possible amount of the
product in a small v.ol'l.lllle. The p.roduct was identified by mass spectroscopic analysis2 • The X-ray pattern was taken and the magnetic susceptibility was also measured. At present the NMR spectra are al!so under investigatioiil.
Keywords
Hrčak ID:
208400
URI
Publication date:
25.11.1962.
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