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Chemical and Biochemical Engineering Quarterly, Vol. 37 No. 2, 2023.

Original scientific paper

https://doi.org/10.15255/CABEQ.2023.2201

Enhancement of Vanillin Partitioning and Recovery in Nanoparticle-based Aqueous Two-phase System Containing PEG and Dextran Polymers

M. Nouri ; Department of Food Science and Technology, Shahr-e-Qods Branch, Islamic Azad University, Tehran, Iran
S. Shahriari orcid id orcid.org/0000-0002-6922-2993 ; Department of Chemical Engineering, Shahr-e-Qods Branch, Islamic Azad University, Tehran, Iran
P. Nabi orcid id orcid.org/0009-0005-4484-3186 ; Department of Chemical Engineering, Science and Research Branch, Islamic Azad University, Tehran, Iran
G. Pazuki ; Department of Chemical Engineering, Amirkabir University of Technology (Tehran Polytechnic), Tehran, Iran

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Abstract

Vanillin, widely utilized in the food, medicinal, and pharmaceutical industries, requires an improved extraction process that is cost-effective and environmentally friendly to meet the growing industrial demand. To tackle this challenge, we conducted an investigation on a nanoparticle-based aqueous two-phase system (ATPS), incorporating polyethylene glycol (PEG) and dextran (DEX). The primary objective was to develop an ATPS that is non-alkaline, operates under mild environmental conditions, and is both non-toxic and cost-effective. The study focused on identifying a suitable nanoparticle that could improve the partitioning of vanillin in ATPS and facilitate economically favorable separation processes. Various nanoparticles were evaluated as additives to enhance vanillin partitioning. The study explores the influence of parameters, such as polymer weight percentages and DEX molecular weight on vanillin partitioning and recovery percentage. Additionally, the impact of incorporating different nanoparticles was assessed in the optimized system composed of 6.5 wt% PEG6000 and 7.8 wt% DEX15000. Results indicate that the addition of only 0.001 g of silver nanoparticles to the optimal system improved the partition coefficient by 42 % and the vanillin recovery percentage by approximately 8 % compared to the nanoparticle-free ATPS.







This work is licensed under a Creative Commons Attribution 4.0 International License.

Keywords

vanillin; polyethylene glycol; dextran; aqueous two-phase system; nanoparticle; partitioning

Hrčak ID:

305242

URI

https://hrcak.srce.hr/305242

Publication date:

2.7.2023.

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