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Original scientific paper

Correction of Preferential Crystallite Orientation in X-ray Quantitative Analysis. Quantitative X:ray Determination of Ca (OH)2

A. Bezjak ; Research Department, Association of Yugoslav Cement Producers, Zagreb , Croatia, Yugoslavia
I. Jelenić ; Research Department, Association of Yugoslav Cement Producers, Zagreb , Croatia, Yugoslavia


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Abstract

The work deals with the problem of preferential orientation
of crystallites in quantitafrwe X-ray analysis. A n ew method has
been worked out theoretically. and practically for the correction
of reflection intensities from 'polycrystalline samples w ith preferentially
oriented crystallites. Equations are included for the
determination of correction parameters. Practical a pplication of
the new method is demonstrated on quantitative X-ray analysis of
calcium hydroxide. The work includes a calibration graph for the
determination of coefficient a, comparing corrected and uncorrecte
d values of analytical intensities of Ca(OH)2.

Keywords

Hrčak ID:

208196

URI

https://hrcak.srce.hr/208196

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