Technical gazette, Vol. 28 No. 5, 2021.
Original scientific paper
https://doi.org/10.17559/TV-20200825223809
Conventional and Non-conventional Sintering Techniques of High Purity Alumina Ceramics
Ivana Ropuš*
; Energo attest zaštita d.o.o., Potočnjakova 4, Zagreb, Croatia
Lidija Ćurković
; Faculty of Mechanical Engineering and Naval Architecture, University of Zagreb, Ivana Lučića 5, Zagreb, Croatia
Vilko Mandić
; Faculty of Chemical Engineering and Technology, University of Zagreb, Marulićev trg 20, 10000 Zagreb, Croatia
Mihone Kerolli Mustafa
; International Business College Mitrovica Str. Bislim Bajgorann, 40000 Mitrovica, Kosovo
Ivana Gabelica
; Faculty of Mechanical Engineering and Naval Architecture, University of Zagreb, Ivana Lučića 5, Zagreb, Croatia
Abstract
The goal of this study is to compare the properties of cold isostatically pressed (CIP) alumina (A2O3) samples sintered by conventional (electrical) and non-conventional (hybrid microwave) techniques. X-ray diffraction was used to determine phase composition of A2O3 samples (raw powder and granules). Thermogravimetric analysis (TGA) and differential thermal analysis (DTA) were used to investigate the thermal behaviour of the Al2O3 powder and granules during the thermal treatment. Compaction of spray dried A2O3 granules into green compact bodies was performed by CIP, followed by sintering of green bodies at 1600 °C in an electrical and hybrid microwave kiln, respectively. Scanning electron microscopy (SEM) was used to analyse morphology of the Al2O3 granules and fracture surface of Al2O3 compacts derived by both sintering techniques. Higher linear shrinkage and densification were obtained for alumina samples sintered in electrical kiln (conventional method), while sintering by faster and more energy efficient hybrid microwave kiln (non-conventional sintering method) yielded alumina samples with finer grain size. Alumina samples sintered by electrical kiln displayed higher relative densities and lower porosities.
Keywords
alumina ceramics; conventional sintering; hybrid microwave sintering; shrinkage
Hrčak ID:
261326
URI
Publication date:
15.8.2021.
Visits: 1.764 *