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https://doi.org/10.5562/cca2339

Synthesis, Crystal and Molecular Structure of Novel Adamantyl Derivatives of N-Aryl Substituted 3-Hydroxy-2-methylpyridine-4-ones

Vesna Petrović Peroković ; Department of Chemistry, Faculty of Science, University of Zagreb, Horvatovac 102a, HR-10000 Zagreb, Croatia
Biserka Prugovečki ; Department of Chemistry, Faculty of Science, University of Zagreb, Horvatovac 102a, HR-10000 Zagreb, Croatia
Željka Car ; Department of Chemistry, Faculty of Science, University of Zagreb, Horvatovac 102a, HR-10000 Zagreb, Croatia

Puni tekst: engleski, pdf (3 MB) str. 317-323 preuzimanja: 745* citiraj
APA 6th Edition
Petrović Peroković, V., Prugovečki, B. i Car, Ž. (2013). Synthesis, Crystal and Molecular Structure of Novel Adamantyl Derivatives of N-Aryl Substituted 3-Hydroxy-2-methylpyridine-4-ones. Croatica Chemica Acta, 86 (3), 317-323. https://doi.org/10.5562/cca2339
MLA 8th Edition
Petrović Peroković, Vesna, et al. "Synthesis, Crystal and Molecular Structure of Novel Adamantyl Derivatives of N-Aryl Substituted 3-Hydroxy-2-methylpyridine-4-ones." Croatica Chemica Acta, vol. 86, br. 3, 2013, str. 317-323. https://doi.org/10.5562/cca2339. Citirano 23.02.2020.
Chicago 17th Edition
Petrović Peroković, Vesna, Biserka Prugovečki i Željka Car. "Synthesis, Crystal and Molecular Structure of Novel Adamantyl Derivatives of N-Aryl Substituted 3-Hydroxy-2-methylpyridine-4-ones." Croatica Chemica Acta 86, br. 3 (2013): 317-323. https://doi.org/10.5562/cca2339
Harvard
Petrović Peroković, V., Prugovečki, B., i Car, Ž. (2013). 'Synthesis, Crystal and Molecular Structure of Novel Adamantyl Derivatives of N-Aryl Substituted 3-Hydroxy-2-methylpyridine-4-ones', Croatica Chemica Acta, 86(3), str. 317-323. https://doi.org/10.5562/cca2339
Vancouver
Petrović Peroković V, Prugovečki B, Car Ž. Synthesis, Crystal and Molecular Structure of Novel Adamantyl Derivatives of N-Aryl Substituted 3-Hydroxy-2-methylpyridine-4-ones. Croatica Chemica Acta [Internet]. 2013 [pristupljeno 23.02.2020.];86(3):317-323. https://doi.org/10.5562/cca2339
IEEE
V. Petrović Peroković, B. Prugovečki i Ž. Car, "Synthesis, Crystal and Molecular Structure of Novel Adamantyl Derivatives of N-Aryl Substituted 3-Hydroxy-2-methylpyridine-4-ones", Croatica Chemica Acta, vol.86, br. 3, str. 317-323, 2013. [Online]. https://doi.org/10.5562/cca2339

Sažetak
Two novel potentially bioactive compounds, esters 2-methyl-1-phenylpyridine-4-one-3-yl adamantan-1-ylethanoate (1) and 1-(p-methoxyphenyl)-2-methylpyridine-4-one-3-yl adamantan-1-ylethanoate (2), were synthesized by esterification of adamantan-1-ylacetic acid with appropriate N-aryl substituted 3-hydroxypyridine-4-one derivatives. Both compounds are fully characterized using standard spectroscopic methods. Crystal and molecular structures of 1 and 2 were determined by the single crystal X-ray diffraction method. The crystal packing of both 1 and 2 shows separation of the hydrophobic and hydrophilic regions. The crystal structure of 1 is characterized by the two-dimensional hydrogen bonding layers parallel to (001). The crystal packing of 2 is characterized by hydrogen-bonded chains extended in the direction [010].(doi: 10.5562/cca2339)

Ključne riječi
adamantan-1-ylacetic acid; 3-hydroxypyridine-4-ones; single crystal X-ray diffraction; Steglich esterification

Hrčak ID: 111643

URI
https://hrcak.srce.hr/111643

Posjeta: 984 *