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Crystal and Molecular Structure of (S)-a-(p-Bromobenzenesulphonamido)-B-propiothiolactone

Ivanka Matijašić ; Laboratory of Organic Chemistry and Biochemistry, Faculty of Science, University of Zagreb, Strossmayerov trg 14, 41000 Zagreb
Giovanni D. Andreetti ; Istituto di Strutturistica Chimica, Universita di Parma, C.N.R., Centro di Studio per la Strutturistica Diffrattometrica, Parma, Italy
Paolo Sgarabotto ; Istituto di Strutturistica Chimica, Universita di Parma, C.N.R., Centro di Studio per la Strutturistica Diffrattometrica, Parma, Italy
Aleksandar Bezjak ; Department of Chemistry, Faculty of Pharmacy and Biochemistry, University of Zagreb, Zagreb
Dragutin Fleš ; Research and Development Institute INA, Zagreb, Yugoslavia

Puni tekst: engleski, pdf (9 MB) str. 621-628 preuzimanja: 40* citiraj
APA 6th Edition
Matijašić, I., Andreetti, G.D., Sgarabotto, P., Bezjak, A. i Fleš, D. (1984). Crystal and Molecular Structure of (S)-a-(p-Bromobenzenesulphonamido)-B-propiothiolactone. Croatica Chemica Acta, 57 (4), 621-628. Preuzeto s https://hrcak.srce.hr/194130
MLA 8th Edition
Matijašić, Ivanka, et al. "Crystal and Molecular Structure of (S)-a-(p-Bromobenzenesulphonamido)-B-propiothiolactone." Croatica Chemica Acta, vol. 57, br. 4, 1984, str. 621-628. https://hrcak.srce.hr/194130. Citirano 04.04.2020.
Chicago 17th Edition
Matijašić, Ivanka, Giovanni D. Andreetti, Paolo Sgarabotto, Aleksandar Bezjak i Dragutin Fleš. "Crystal and Molecular Structure of (S)-a-(p-Bromobenzenesulphonamido)-B-propiothiolactone." Croatica Chemica Acta 57, br. 4 (1984): 621-628. https://hrcak.srce.hr/194130
Harvard
Matijašić, I., et al. (1984). 'Crystal and Molecular Structure of (S)-a-(p-Bromobenzenesulphonamido)-B-propiothiolactone', Croatica Chemica Acta, 57(4), str. 621-628. Preuzeto s: https://hrcak.srce.hr/194130 (Datum pristupa: 04.04.2020.)
Vancouver
Matijašić I, Andreetti GD, Sgarabotto P, Bezjak A, Fleš D. Crystal and Molecular Structure of (S)-a-(p-Bromobenzenesulphonamido)-B-propiothiolactone. Croatica Chemica Acta [Internet]. 1984 [pristupljeno 04.04.2020.];57(4):621-628. Dostupno na: https://hrcak.srce.hr/194130
IEEE
I. Matijašić, G.D. Andreetti, P. Sgarabotto, A. Bezjak i D. Fleš, "Crystal and Molecular Structure of (S)-a-(p-Bromobenzenesulphonamido)-B-propiothiolactone", Croatica Chemica Acta, vol.57, br. 4, str. 621-628, 1984. [Online]. Dostupno na: https://hrcak.srce.hr/194130. [Citirano: 04.04.2020.]

Sažetak
(S)-a-(p-Bromobenzenesulphonamido)-{J-propiothiolactone,
C9H8N03S2Br, crystallizes in the orthorhombic system with a =
= 1.0125(2), b = 1.2439(1) and c = 0.9304(3) nm, Z = 4 in space group
P212121• The compound is isostructural with the analogous chloro
derivative. The crystal structure has been refined from diffractometer
data to conventional R and Ra values of 0.045 and 0.048 for
2277 reflections with I ~ 2a (I). The heterocyclic four-membered
ring has a puckering angle of 8.9(4) 0
• The dihedral angle between
the best planes of the /)-propiothiolactone and benzene rings is
84.1(2) 0
• The structure consists of discrete molecules connected
along the a axis by intermolecular hydrogen bonds N-H ... O of
291.9(7) pm.

Hrčak ID: 194130

URI
https://hrcak.srce.hr/194130

Posjeta: 71 *