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https://doi.org/10.5562/cca3463

Hydroxyapatite/Silver Nanoparticles Powders as Antimicrobial Agent for Bone Replacements

Agnieszka Sobczak-Kupiec ; Institute of Inorganic Chemistry and Technology, Cracow University of Technology, 31-155 Cracow, Poland
Dagmara Malina ; Institute of Inorganic Chemistry and Technology, Cracow University of Technology, 31-155 Cracow, Poland
Regina Kijkowska ; Institute of Inorganic Chemistry and Technology, Cracow University of Technology, 31-155 Cracow, Poland
Wioletta Florkiewicz ; Institute of Inorganic Chemistry and Technology, Cracow University of Technology, 31-155 Cracow, Poland
Klaudia Pluta ; Institute of Inorganic Chemistry and Technology, Cracow University of Technology, 31-155 Cracow, Poland
Zbigniew Wzorek ; Institute of Inorganic Chemistry and Technology, Cracow University of Technology, 31-155 Cracow, Poland

Puni tekst: engleski, pdf (10 MB) str. 59-68 preuzimanja: 470* citiraj
APA 6th Edition
Sobczak-Kupiec, A., Malina, D., Kijkowska, R., Florkiewicz, W., Pluta, K. i Wzorek, Z. (2019). Hydroxyapatite/Silver Nanoparticles Powders as Antimicrobial Agent for Bone Replacements. Croatica Chemica Acta, 92 (1), 59-68. https://doi.org/10.5562/cca3463
MLA 8th Edition
Sobczak-Kupiec, Agnieszka, et al. "Hydroxyapatite/Silver Nanoparticles Powders as Antimicrobial Agent for Bone Replacements." Croatica Chemica Acta, vol. 92, br. 1, 2019, str. 59-68. https://doi.org/10.5562/cca3463. Citirano 05.03.2021.
Chicago 17th Edition
Sobczak-Kupiec, Agnieszka, Dagmara Malina, Regina Kijkowska, Wioletta Florkiewicz, Klaudia Pluta i Zbigniew Wzorek. "Hydroxyapatite/Silver Nanoparticles Powders as Antimicrobial Agent for Bone Replacements." Croatica Chemica Acta 92, br. 1 (2019): 59-68. https://doi.org/10.5562/cca3463
Harvard
Sobczak-Kupiec, A., et al. (2019). 'Hydroxyapatite/Silver Nanoparticles Powders as Antimicrobial Agent for Bone Replacements', Croatica Chemica Acta, 92(1), str. 59-68. https://doi.org/10.5562/cca3463
Vancouver
Sobczak-Kupiec A, Malina D, Kijkowska R, Florkiewicz W, Pluta K, Wzorek Z. Hydroxyapatite/Silver Nanoparticles Powders as Antimicrobial Agent for Bone Replacements. Croatica Chemica Acta [Internet]. 2019 [pristupljeno 05.03.2021.];92(1):59-68. https://doi.org/10.5562/cca3463
IEEE
A. Sobczak-Kupiec, D. Malina, R. Kijkowska, W. Florkiewicz, K. Pluta i Z. Wzorek, "Hydroxyapatite/Silver Nanoparticles Powders as Antimicrobial Agent for Bone Replacements", Croatica Chemica Acta, vol.92, br. 1, str. 59-68, 2019. [Online]. https://doi.org/10.5562/cca3463

Sažetak
This paper reports a superficial morphological modification of the hydroxyapatite grains obtained by in situ deposition of Ag nanoparticles on natural origin calcium phosphate powder. Ceramic material was prepared in three stage bone treatment, including hydrolysis with a lactic acid, pre-calcination, and proper calcination. Subsequently, the Ag nanoparticles were synthesized by chemical reduction of Ag+ by sodium borohydride in a solution of polyvinylpyrrolidone and in presence of hydroxyapatite. Such-prepared materials were investigated with X-ray diffraction, Fourier-transformed infrared spectroscopy, atomic absorption spectrometry and scanning electron microscopy with energy dispersive spectroscopy. Furthermore, Ca/P molar ratio was calculated and microbiological tests were performed to investigate materials antimicrobial activity. The appearance of Ag nanoparticles located on phosphate surface was confirmed by SEM analysis, and no chemical bonding with hydroxyapatite was recorded by IR and XRD techniques. Additionally, the biological assessment revealed bactericidal effect on Escherichia coli and Staphylococcus aureus, while slightly affected on Enterococcus faecalis viability.

Creative Commons License This work is licensed under a Creative Commons Attribution 4.0 International License.

Ključne riječi
hydroxyapatite; silver nanoparticles; antibacterial activity; surface modification

Hrčak ID: 217460

URI
https://hrcak.srce.hr/217460

Posjeta: 753 *