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Copper(I) Complexes of N-thiophosphorylated Bis-thiourea [CH2NHC(S)NHP(S)(OiPr)2]2 and Phosphines (PPh3, Ph2P(CH2)1–3PPh2, Ph2P(C5H4FeC5H4)PPh2): Versatile Structures and Luminescence

Damir A. Safin ; Institut für Anorganische Chemie, Universität zu Köln, Greinstrasse 6, D-50939 Köln, Germany
Maria G. Babashkina ; Institut für Anorganische Chemie, Universität zu Köln, Greinstrasse 6, D-50939 Köln, Germany
Axel Klein ; Institut für Anorganische Chemie, Universität zu Köln, Greinstrasse 6, D-50939 Köln, Germany

Puni tekst: engleski, pdf (1 MB) str. 353-356 preuzimanja: 958* citiraj
APA 6th Edition
Safin, D.A., Babashkina, M.G. i Klein, A. (2010). Copper(I) Complexes of N-thiophosphorylated Bis-thiourea [CH2NHC(S)NHP(S)(OiPr)2]2 and Phosphines (PPh3, Ph2P(CH2)1–3PPh2, Ph2P(C5H4FeC5H4)PPh2): Versatile Structures and Luminescence. Croatica Chemica Acta, 83 (3), 353-356. Preuzeto s https://hrcak.srce.hr/62214
MLA 8th Edition
Safin, Damir A., et al. "Copper(I) Complexes of N-thiophosphorylated Bis-thiourea [CH2NHC(S)NHP(S)(OiPr)2]2 and Phosphines (PPh3, Ph2P(CH2)1–3PPh2, Ph2P(C5H4FeC5H4)PPh2): Versatile Structures and Luminescence." Croatica Chemica Acta, vol. 83, br. 3, 2010, str. 353-356. https://hrcak.srce.hr/62214. Citirano 06.03.2021.
Chicago 17th Edition
Safin, Damir A., Maria G. Babashkina i Axel Klein. "Copper(I) Complexes of N-thiophosphorylated Bis-thiourea [CH2NHC(S)NHP(S)(OiPr)2]2 and Phosphines (PPh3, Ph2P(CH2)1–3PPh2, Ph2P(C5H4FeC5H4)PPh2): Versatile Structures and Luminescence." Croatica Chemica Acta 83, br. 3 (2010): 353-356. https://hrcak.srce.hr/62214
Harvard
Safin, D.A., Babashkina, M.G., i Klein, A. (2010). 'Copper(I) Complexes of N-thiophosphorylated Bis-thiourea [CH2NHC(S)NHP(S)(OiPr)2]2 and Phosphines (PPh3, Ph2P(CH2)1–3PPh2, Ph2P(C5H4FeC5H4)PPh2): Versatile Structures and Luminescence', Croatica Chemica Acta, 83(3), str. 353-356. Preuzeto s: https://hrcak.srce.hr/62214 (Datum pristupa: 06.03.2021.)
Vancouver
Safin DA, Babashkina MG, Klein A. Copper(I) Complexes of N-thiophosphorylated Bis-thiourea [CH2NHC(S)NHP(S)(OiPr)2]2 and Phosphines (PPh3, Ph2P(CH2)1–3PPh2, Ph2P(C5H4FeC5H4)PPh2): Versatile Structures and Luminescence. Croatica Chemica Acta [Internet]. 2010 [pristupljeno 06.03.2021.];83(3):353-356. Dostupno na: https://hrcak.srce.hr/62214
IEEE
D.A. Safin, M.G. Babashkina i A. Klein, "Copper(I) Complexes of N-thiophosphorylated Bis-thiourea [CH2NHC(S)NHP(S)(OiPr)2]2 and Phosphines (PPh3, Ph2P(CH2)1–3PPh2, Ph2P(C5H4FeC5H4)PPh2): Versatile Structures and Luminescence", Croatica Chemica Acta, vol.83, br. 3, str. 353-356, 2010. [Online]. Dostupno na: https://hrcak.srce.hr/62214. [Citirano: 06.03.2021.]

Sažetak
Reaction of the potassium solution of [CH2NHC(S)NHP(S)(OiPr)2]2 (H2L) with [Cu(PPh3)3I]
or a mixture of CuI and Ph2P(CH2)1–3PPh2 or Ph2P(C5H4FeC5H4)PPh2 in aqueous EtOH/CH2Cl2
leads to binuclear [Cu2(PPh3)2L] (1), [Cu2(Ph2PCH2PPh2)L] (2), [Cu2{Ph2P(CH2)2PPh2}2L] (3),
[Cu2{Ph2P(CH2)3PPh2}2L] (4) or [Cu2{Ph2P(C5H4FeC5H4)PPh2}2L] (5) complexes. The structures of these
compounds were investigated by IR, 1H and 31P{1H} NMR spectroscopy; their compositions were
examined by microanalysis. The luminescent properties of complexes 1–5 in the solid state are reported.

Ključne riječi
coordination chemistry; copper(I); thiophosphorylthiourea; phosphine; luminescence

Hrčak ID: 62214

URI
https://hrcak.srce.hr/62214

Posjeta: 1.207 *