Acta Pharmaceutica, Vol. 68 No. 1, 2018.
Izvorni znanstveni članak
https://doi.org/10.2478/acph-2018-0003
Distinguishing Smilax glabra and Smilax china rhizomes by flow-injection mass spectrometry combined with principal component analysis
JIAN LIANG
; Jiangxi University of Traditional Chinese Medicine, Nanchang, 330004, China
MENG ZHOU
; Jiangxi University of Traditional Chinese Medicine, Nanchang, 330004, China
LIN-YU LI
; Jiangxi University of Traditional Chinese Medicine, Nanchang, 330004, China
JI-CHENG SHU
; Jiangxi University of Traditional Chinese Medicine, Nanchang, 330004, China
YONG-HONG LIANG
; Jiangxi University of Traditional Chinese Medicine, Nanchang, 330004, China
FENG-QIN LI
; Jiangxi University of Traditional Chinese Medicine, Nanchang, 330004, China
LI XIONG
; Jiangxi Province Center for Disease Control and Prevention, Nanchang, 330029, China
HUI-LIAN HUANG
; Jiangxi University of Traditional Chinese Medicine, Nanchang, 330004, China
Sažetak
Flow-injection mass spectrometry (FIMS) coupled with a chemometric method is proposed in this study to profile and distinguish between rhizomes of Smilax glabra (S. glabra) and Smilax china (S. china). The proposed method employed an electrospray-time-of-flight MS. The MS fingerprints were analyzed using principal component analysis (PCA) and orthogonal partial least squares discriminant analysis (OPLS-DA) with the aid of SIMCA software. Findings showed that the two kinds of samples perfectly fell into their own classes. Further predictive study showed desirable predictability and the tested samples were successfully and reliably identified. The study demonstrated that the proposed method could serve as a powerful tool for distinguishing between S. glabra and S. china.
Ključne riječi
Smilax glabra; Smilax china; rhizome; flow injection; mass spectrometry; PCA; OPLS-DA
Hrčak ID:
189691
URI
Datum izdavanja:
31.3.2018.
Posjeta: 1.635 *