Croatica Chemica Acta, Vol. 27 No. 4, 1955.
Izvorni znanstveni članak
Synthesis of 1-Aminoheneicosane
N. Ž. Stanaćev
; Department of Chemistry, Medical Faculty, University of Zagreb, Croatia, Yugoslavia
M. Proštenik
; Department of Chemistry, Medical Faculty, University of Zagreb, Croatia, Yugoslavia
Sažetak
1-Aminoheneicosane [V] was prepared by the condensation of dibenzyl sodiotetradecylmalonate with E-phthaloylaminocaproic acid chloride [III]. Following substances are described: 1. E-Phthaloylaminocaproic acid [II], m. p. 107°; 2. E-phthaloylaminocaproic acid chloride [III], b. p. 175-1780 at '1.2 mm.; 3. 1-phthaloylamino-6-heneicosanone [IV], m. p. 83-84°; oxime, m. p. 59-60°; 4. 1-aminoheneicosane [VJ, m. p. 93-94°; oxalate, m. p. 170-172° (decomp.); 5. 1-benzoylamino-6-heneicosanone, m. p. 94--95°.
Ključne riječi
Hrčak ID:
247908
URI
Datum izdavanja:
1.2.1956.
Posjeta: 499 *