Metallurgy, Vol. 61 No. 2, 2022.
Preliminary communication
Extraction of amorphous silica from waste dust of electrowinning of ilmenite concentrate
A. A. Ultarakova
orcid.org/0000-0001-9428-8508
; Satbayev University, “Institute of Metallurgy and Ore Beneficiation” JSC, Almaty, Kazakhstan
Z. B. Karshigina
; Satbayev University, “Institute of Metallurgy and Ore Beneficiation” JSC, Almaty, Kazakhstan
N. G. Lokhova
; Satbayev University, “Institute of Metallurgy and Ore Beneficiation” JSC, Almaty, Kazakhstan
A. M. Yessengaziyev
orcid.org/0000-0002-4989-4119
; Satbayev University, “Institute of Metallurgy and Ore Beneficiation” JSC, Almaty, Kazakhstan
K. K. Kassymzhanov
; Satbayev University, “Institute of Metallurgy and Ore Beneficiation” JSC, Almaty, Kazakhstan
S. S. Tolegenova
; Satbayev University, “Institute of Metallurgy and Ore Beneficiation” JSC, Almaty, Kazakhstan
Abstract
The paper presents research on the processing of waste dust from the electrical smelting of ilmenite concentrates with the removal of silicon from them by the fluoride method. The optimum conditions for fluorination of electric smelting dust were determined, at which the degree of silicon fluoride sublimation was 84,2 %. The silicon-containing sublime obtained in the presence of an ammonia agent has been studied. Based on the results of thermal analysis and studies on the effect of process duration the optimum pyrolysis modes that provide the separation of fluoride and silicon oxide: temperature 530 - 560 °C and duration of 60 - 80 min have been determined. The content of silicon oxide in the obtained product was 96,3 %.
Keywords
extraction; amorphous silica; dust; phase analysis; X-ray research
Hrčak ID:
265927
URI
Publication date:
1.4.2022.
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