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Kemija u industriji : Časopis kemičara i kemijskih inženjera Hrvatske, Vol. 69 No. 9-10 (special issue), 2020.

Pregledni rad

https://doi.org/10.15255/KUI.2020.020

The Application of Headspace Solid-phase Microextraction as a Preparation Approach for Gas Chromatography with Mass Spectrometry

Igor Jerković ; Sveučilište u Splitu, Kemijsko-tehnološki fakultet, Zavod za organsku kemiju, R. Boškovića 35, 21 000 Split
Zvonimir Marijanović orcid id orcid.org/0000-0001-9786-5956 ; Sveučilište u Splitu, Kemijsko-tehnološki fakultet, Zavod za prehrambenu tehnologiju i biotehnologiju, R. Boškovića 35, 21 000 Split
Ani Radonić orcid id orcid.org/0000-0003-2744-9441 ; Sveučilište u Splitu, Kemijsko-tehnološki fakultet, Zavod za prehrambenu tehnologiju i biotehnologiju, R. Boškovića 35, 21 000 Split
Marina Zekić ; Sveučilište u Splitu, Kemijsko-tehnološki fakultet, Zavod za organsku kemiju, R. Boškovića 35, 21 000 Split
Marina Kranjac orcid id orcid.org/0000-0001-8567-9742 ; Sveučilište u Splitu, Kemijsko-tehnološki fakultet, Zavod za organsku kemiju, R. Boškovića 35, 21 000 Split

Puni tekst: engleski pdf 217 Kb

str. 515-520

preuzimanja: 455

citiraj

Sažetak

Reviewed in brief are the selected results of the application of headspace solid-phase microextraction as a preparative approach for gas chromatography – mass spectrometry (HS-SPME/GC-MS) for natural organic compounds research at the University of Split, Faculty of Chemistry and Technology. A wide variety of headspace compounds from different natural sources has been identified: lower aliphatic compounds (e.g., C5- and C6-compounds), aromatic compounds, monoterpenes (e.g., linalool derivatives (oxides, anhydro-oxides, epoxides), hotrienol), sesquiterpenes (e.g., eudesmol isomers, hydrocarbons), and C9- and C13-norisoprenoids (e.g., 3,4-dihydro-3-oxoedulan, 4-oxoisophorone, trans-β-damascenone). These compounds are important phytochemicals as flavour/fragrance compounds, chemical markers of the botanical origin or others (e.g., allelochemicals, pheromones, or acaricide residue).




This work is licensed under a Creative Commons Attribution 4.0 International License.

Ključne riječi

headspace solid-phase microextraction (HS-SPME); gas chromatography and mass spectrometry (GC-MS); lower aliphatic compounds; aromatic compounds; monoterpenes; sesquiterpenes; C9- and C13-norisoprenoids

Hrčak ID:

243912

URI

https://hrcak.srce.hr/243912

Datum izdavanja:

24.9.2020.

Podaci na drugim jezicima: hrvatski

Posjeta: 1.269 *