Pregledni rad
https://doi.org/10.15255/KUI.2020.020
The Application of Headspace Solid-phase Microextraction as a Preparation Approach for Gas Chromatography with Mass Spectrometry
Igor Jerković
; Sveučilište u Splitu, Kemijsko-tehnološki fakultet, Zavod za organsku kemiju, R. Boškovića 35, 21 000 Split
Zvonimir Marijanović
orcid.org/0000-0001-9786-5956
; Sveučilište u Splitu, Kemijsko-tehnološki fakultet, Zavod za prehrambenu tehnologiju i biotehnologiju, R. Boškovića 35, 21 000 Split
Ani Radonić
orcid.org/0000-0003-2744-9441
; Sveučilište u Splitu, Kemijsko-tehnološki fakultet, Zavod za prehrambenu tehnologiju i biotehnologiju, R. Boškovića 35, 21 000 Split
Marina Zekić
; Sveučilište u Splitu, Kemijsko-tehnološki fakultet, Zavod za organsku kemiju, R. Boškovića 35, 21 000 Split
Marina Kranjac
orcid.org/0000-0001-8567-9742
; Sveučilište u Splitu, Kemijsko-tehnološki fakultet, Zavod za organsku kemiju, R. Boškovića 35, 21 000 Split
Sažetak
Reviewed in brief are the selected results of the application of headspace solid-phase microextraction as a preparative approach for gas chromatography – mass spectrometry (HS-SPME/GC-MS) for natural organic compounds research at the University of Split, Faculty of Chemistry and Technology. A wide variety of headspace compounds from different natural sources has been identified: lower aliphatic compounds (e.g., C5- and C6-compounds), aromatic compounds, monoterpenes (e.g., linalool derivatives (oxides, anhydro-oxides, epoxides), hotrienol), sesquiterpenes (e.g., eudesmol isomers, hydrocarbons), and C9- and C13-norisoprenoids (e.g., 3,4-dihydro-3-oxoedulan, 4-oxoisophorone, trans-β-damascenone). These compounds are important phytochemicals as flavour/fragrance compounds, chemical markers of the botanical origin or others (e.g., allelochemicals, pheromones, or acaricide residue).
This work is licensed under a Creative Commons Attribution 4.0 International License.
Ključne riječi
headspace solid-phase microextraction (HS-SPME); gas chromatography and mass spectrometry (GC-MS); lower aliphatic compounds; aromatic compounds; monoterpenes; sesquiterpenes; C9- and C13-norisoprenoids
Hrčak ID:
243912
URI
Datum izdavanja:
24.9.2020.
Posjeta: 1.880 *